| 2 | Synthesis of Water-Soluble Chitosan From Squid Pens Waste for Capsule Shell Materials显示文摘Water-Soluble Chitosan(WSC)has been sucessfuly synthesized from squid pens waste.The synthesis of chitosan from chitin was carried out by optimization of deacetylation temperature and time.Chitin was obtained from squid pens waste by demineralization and deproteinization process.HCl 7%was used for demineralization and NaOH 10%at 60℃ was applied for deproteinization process.Deacetylation reaction was carried out at varied temperatures i.e.,60℃,70℃,80℃,90℃ and 100℃ in NaOH 50%solution for 10 hours.Deacetylation reaction time were varied for 2 hours,4 hours,6 hours,8 hours,and 10 hours.The crude chitosan obtained then reacted with H2O230%to depolymerize.The synthesis product obtained then characterized by FTIR.The result of squid chitin yield was 33.9%.The optimum temperature and time of chitosan deacetylation process were 90℃ for 8 hours as indicated by the value of deacetylation degree(DD)that equal to 83.94%at optimum temperature and 82.22%at optimum reaction time.The percentage of WSC yield at optimum temperature(90℃)and optimum time(8 hours)were 27.59%and 23.16%,respectively.WSC solubility test was done in water and HCl 0,1N.The solubility of 2.8325 mg/mL and 0.8125 mg/mL were obtained in acid medium and water medium,respectively. | Malinda Syifa Yusharani Stenley Harmami Ita Ulfin Suprapto Suprapto Yatim Lailun Ni’mah | 2019 | Journal of Renewable Materials2019，7，7： | 0 |
| 3 | The Fabrication of Water-Soluble Chitosan Capsule Shell Modified by Alginate and Gembili Starch(Dioscorea esculenta L)显示文摘Capsule shells have been successfully fabricated from water-soluble chitosan(WSC)with the addition of alginate and Gembili starch.WSC was synthesized from crab shell chitosan by depolymerization reaction.The capsule shells were made with the composition of WSC:Alginate,2:1,3:1 and 4:1(w/w)with and without the addition of Gembili starch.Gembili starch was added with a ratio of Alginate:Starch,1:1(w/w).The capsule shell properties were evaluated according to Indonesian Pharmacopoeia standard.The solubility test showed that the capsule shells were comply with the standard.The highest degrees of swelling in water and HCl 0.1 N solution were 491.93%and 410.51%,respectively.The highest degradation percentages in water and HCl 0.1 N solution were 57.80%and 21.44%,respectively.The observation of physical appearance indicated that the capsule shell with WSC:Alginate:Starch in ratio of 3:1:1 has appearance close to commercial capsule shell. | Yatim Lailun Ni’mah Suprapto Suprapto Harmami Ita Ulfin Puput Asmaul Fauziyah | 2022 | Journal of Renewable Materials2022，10，9： | 0 |
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