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| 1 | Effect of C and Hf Contents on the Interface Reactions and Wettability between a Ni_3Al-Based Superalloy and Ceramic Mould Material显示文摘The influence of active elements C and Hf on the interface reactions and wettability between a Ni_3Albased superalloy and the ceramic mould material was studied by using a sessile drop experiment.The microstructure of the alloy interface was investigated by scanning electron microscopy analysis and the phase identification was performed by X-ray diffraction analysis.The results show that interface reactions occur as C and Hf contents reach a critical value.The critical values for C and Hf to cause interface reactions are 0.12 wt%and 1.17 wt%,respectively.The reaction products contain HfO_2 and 9Al_2O_3-Cr_2O_3.Adsorptions of Hf and interface reactions improve the wettability obviously. | Xiaoyan Chen Yizhou Zhou Tao Jin Xiaofeng Sun | 2016 | Journal of Materials Science & Technology2016，32，2： | 8 |
| 2 | Fate of antibiotics and antibiotic resistance genes in a full-scale restaurant food waste treatment plant:Implications of the roles beyond heavy metals and mobile genetic elements显示文摘Is our food safe and free of the crisis of antibiotics and antibiotic resistance (AR)?And will the derived food waste (FW) impose AR risk to the environment after biological treatment? This study used restaurant FW leachates flowing through a 200 tons-waste/day biological treatment plant as a window to investigate the fate of antibiotics and antibiotic-resistance genes (ARGs) during the acceptance and treatment of FW.Sulfonamides (sulfamethazine,sulfamethoxazole) and quinolones (ciprofloxacin,enrofloxacin,ofloxacin) were detected during FW treatment,while tetracyclines,macrolides and chloramphenicols were not observable.ARGs encoding resistance to sulfonamides,tetracyclines and macrolides emerged in FW leachates.Material flow analysis illustrated that the total amount of antibiotics (except sulfamethazine) and ARGs were constant during FW treatment processes.Both the concentration and total amount of most antibiotics and ARGs fluctuated during treatment,physical processes (screening,centrifugation,solid-liquid and oil-water separation) did not decrease antibiotic or ARGs concentrations or total levels permanently;the affiliated wastewater treatment plant appeared to remove sulfonamides and most ARGs concentrations and total amount.Heavy metals Ni,Co and Cu were important for disseminating antibiotics concentrations and MGEs for distributing ARGs concentrations.Humic substances (fulvic acids,hydrophilic fractions),C-associated and N-associated contents were essential for the distribution of the total amounts of antibiotics and ARGs.Overall,this study implied that human food might not be free of antibiotics and ARGs,and FW was an underestimated AR pool with various determinants.Nonetheless,derived hazards of FW could be mitigated through biological treatment with well-planned daily operations. | Pinjing He Zhuofeng Yu Liming Shao Yizhou Zhou Fan Lü | 2019 | Journal of Environmental Sciences2019，31，11： | 7 |
| 3 | Influence of Temperature and Salinity on Germination of Eelgrass (Zostera marina L.) Seeds显示文摘Seagrass restoration as part of ocean ecosystem protection has been launched for many years all over the world, but intensive research on this subject in China has just begun in recent years. Seed broadcasting has been widely accepted as the most potentially useful method for seagrass restoration over large areas. We examined the influence of key environmental factors on seed germination to help promote eelgrass bed restoration. Under anoxic conditions, the influence of temperature and salinity on the germination rate of eelgrass (Zostera marina L.) seeds was examined at different combinations of four temperatures (4, 9, 14, and 24℃) and nine salinities (5 to 45, increment of 5). The effect of significant interaction of temperature and salinity on germination rate was observed (ANOVA) (P<0.001). The highest germination rate (83.3 ± 3.5)% was reached in 8 weeks at 14℃ and salinity 5. Higher temperature significantly increased the germination rate at salinity 5 (P<0.001) during the whole observation period except for 24℃, while lower salinity significantly increased the germination rate at 14℃ (P<0.001). Although significant interaction was found between temperature and salinity (P<0.001), the influence of salinity was stronger than that of temperature for the germination of eelgrass seeds. These results provide useful information for the propagation of artificial seedlings for seagrass restoration in China. | PAN Jinhua JIANG Xin LI Xiaojie CONG Yizhou ZHANG Zhuangzhi LI Zhiling ZHOU Weili HAN Houwei LUO Shiju YANG Guanpin | 2011 | Journal of Ocean University of China2011，10，2： | 7 |
| 4 | MiR-29a/b/c regulate human circadian gene hPER1 expression by targeting its 3/UTR显示文摘在哺乳动物的几必要生物进步被生理节奏的节奏调整。不过分子的机制 ofoscillating 这些生理节奏的节奏被揭开了,生理节奏的基因的特定的功能不是很, clear.It 被报导了那由 microRNA 将生理节奏的基因击倒是有用策略探索 circadianrhythms 的功能。在这研究,通过屏蔽途径的前面的生物信息学,我们作为有势力 inhibitorsfor 识别了 miR-29a/b/c 人的生理节奏的基因 hPER1。我们进一步发现 miR-29a/b/c 能直接在人的 A549 房间在 mRNA 和蛋白质表示层次指向 hPER1 3untranslated 区域(UTR ) 和下面调整 hPER1。因此,我们的调查结果建议 hPER1 的表示被 miR-29a/b/c 调整,它可以也为 hPER1 的功能提供新线索。 | Xiyan Zhao Xueqiang Zhu Shuting Cheng Yizhou Xie Zhengrong Wang Yanyou Liu Zhou Jiang Jing Xiao Huiling Guo Yuhui Wang | 2014 | Acta Biochimica et Biophysica Sinica2014，46，4： | 7 |
| 5 | Microstructure and tensile properties of DD32 single crystal Ni-base superalloy repaired by laser metal forming显示文摘In this work,the microstructure and tensile properties of DD32 single-crystal(SC)superalloy repaired by laser metal forming(LMF)using pulsed laser have been studied in detail.The microstructures of the deposited samples and the tensile-ruptured samples were characterized by optical microscopy(OM),transmission electron microscope(TEM)and scanning electron microscope(SEM).Due to high cooling rate,the primary dendrite spacing in the deposited area(17.2μm)was apparently smaller than that in the substrate area(307μm),and the carbides in the deposited samples were also smaller compared with that in the substrate area.The formation of(γ+γ’)eutectic in the initial layer of repaired SC was inhibited because of the high cooling rate.As the deposition proceeded,the cooling rate decreased,and the(γ+γ’)eutectic increased gradually.The(γ+γ’)eutectic at heat-affected zone(HAZ)in the molten pool dissolved partly because of the high temperature at HAZ,but there were still residual eutectics.Tensile test results showed that tensile behavior of repaired SC at different temperatures was closely related to the MC carbides,solidification porosity,γ’phase,and(γ+γ’)eutectic.At moderate temperature,the samples tested fractured preferentially at the substrate area due to the fragmentation of the coarse MC carbide in the substrate area.At elevated temperature,the(γ+γ’)eutectic and solidification porosity in the deposited area became the source of cracks,which deteriorated the high-temperature properties and made the samples rupture at the deposited area preferentially. | Shiwei Ci Jingjing Liang Jinguo Li Yizhou Zhou Xiaofeng Sun | 2020 | Journal of Materials Science & Technology2020，42，10： | 6 |
| 6 | Effects of scanning speed on microstructure in laser surface-melted single crystal superalloy and theoretical analysis显示文摘Scanning speed is a critical parameter for laser process,which can play a key role in the microstructure evolution of laser melting.In the laser melting of single crystal superalloy,the effects of scanning speed were investigated by experimental analysis and computational simulation.The laser was scanning along710 direction on(001) surface in different speeds.Solidification microstructures of dendrites growth direction and the primary dendritic spacing were analyzed by metallograph.Besides,a planar interface during solidification was taken into attention.Experiment results indicated that the primary dendritic spacing and thickness of planar interface decrease with the increase of speed.Through simulation,distribution of dendrites growth velocity and thermal gradient along dendrite growth direction were calculated,and the simulation of dendrites growth direction agreed with the experiment results.Additionally,a constant value was acquired which can be used to predict the primary dendritic spacing.Moreover,according to curve-fitting method and inequality relation,a model was proposed to predict the thickness of planar interface. | Guowei Wang Jingjing Liang Yanhong Yang Yu Shi Yizhou Zhou Tao Jin Xiaofeng Sun | 2018 | Journal of Materials Science & Technology2018，34，8： | 5 |
| 7 | Balancing flexural strength and porosity in DLP-3D printing Al_(2)O_(3)cores for hollow turbine blades显示文摘High porosity and high strength are usually mutually exclusive in the preparation of ceramic materials.However,high porosity and flexural strength are required for the preparation of complex ceramic cores for hollow turbine blades.In this study,Al_(2)O_(3)cores with high porosity and high flexural strength were successfully prepared using digital light processing(DLP)3 D printing technology.The influence of sintering temperature on the microstructure,pore evolution,and flexural strength of the cores were investigated.With an increase in the sintering temperature,the porosity of the ceramic cores first increased and then decreased,reaching a maximum value of 35%at 1400℃.The flexural strength increased with the increase in sintering temperature,but at 1400℃the incremental enhancement of flexural strength was greatest.Combined with the core service requirements and core performance,this study selected 1400℃(open porosity of 35.1%and flexural strength of 20.3 MPa)as the optimal sintering temperature for the DLP-3 D printed Al_(2)O_(3)core. | Qiaolei Li Xiaolong An Jingjing Liang Yongsheng Liu Kehui Hu Zhigang Lu Xinyan Yue Jinguo Li Yizhou Zhou Xiaofeng Sun | 2022 | Journal of Materials Science & Technology2022，，9： | 4 |
| 8 | Dendritic Growth Pattern and Dendritic Network Distortion in the Platform of a Ni-based Superalloy显示文摘The pattern of dendritic growth and distortion of dendritic network in the platform have been investigated by one mold casting with different platform length during directional solidification. As the platform length elongates, the symmetry of dendritic growth along left and right edges gradually worsens in platform base. While the platform length reaches 14 mm, the distortion of dendritic network is first observed in outward platform. It is found that the distortion of dendritic network along platform inside is more serious than that along platform edges. Both[001] deviation and accumulated misorientation along platform inside, up to 9 and 16.3, respectively, are far greater than those along lefte outwarde right edges. The deformation of dendritic network in a platform may be caused by the asymmetry of the solidification front at the mush zone. | Xiaoli Zhang Yizhou Zhou Yanyun Han Tao Jin Xiaofeng Sun | 2014 | Journal of Materials Science & Technology2014，30，3： | 4 |
| 9 | The interaction and migration of deformation twin in an eutectic high-entropy alloy AlCoCrFeNi2.1显示文摘An eutectic high-entropy alloy consisting Al, Co, Cr, Fe and Ni elements was prepared by vacuum directional solidification technology. The alloy exhibits excellent comprehensive mechanical performance during tension at temperature range of 600–700℃. The microstructure reveals the intersection of twintwin is the prevailing deformation mechanism and the twins play a dual role in strengthening and toughening the alloy in the thermomechanical process. The deformation twin variants I and were formed by the edge dislocation 112 and the mixed dislocation 211 on the {111} crystal planes, respectively. Besides, the dislocation jogs and kinks caused by twin intersection on the slip planes can strengthen the alloy, which may contribute to the high strength(the tensile strengths at the 600°and 700°tensile tests are respectively780 MPa and 630 MPa.). Moreover, the coherent twin boundary migration has the function of coordinating deformation and contributes to the high ductility of the alloy. | Yaoli Zhang Jinguo Li Xinguang Wang Yiping Lu Yizhou Zhou Xiaofeng Sun | 2019 | Journal of Materials Science & Technology2019，35，5： | 4 |
| 10 | Effect of solidification rate on competitive grain growth in directional solidification of a nickel-base superalloy显示文摘The mechanism of grain structure evolution during directional solidification is a fundamental subject in material science. Within the published research there exist conflicting views on the mechanism of grain overgrowth. To study the effect of solidification rate on grain structure evolution, bi-crystals samples were produced in a nickel-base superalloy at different solidification rates. It was found that at the convergent grain boundaries those grains better aligned with respect to the heat flux more readily overgrew neighbouring grains with misaligned orientations and the effect became more pronounced as solidification rate was increased. However, at diverging grain boundaries the rate of overgrowth was invariant to the solidification rate. These experimental results were compared with models in the literature. Thus, a better insight into competitive grain growth in directional solidification processes was obtained. | ZHOU YiZhou SUN XiaoFeng | 2012 | Science China(Technological Sciences)2012，55，5： | 4 |
| 11 | Microstructure of Carbides at Grain Boundaries in Nickel Based Superalloys显示文摘It is well known that carbides at grain boundaries play an important role in affecting mechanical properties of nickel based superalloys. In order to deeply understand the relationship between grain boundary structures and properties, in this work, we have investigated the microstructure of grain boundaries with different misorientation angles in bicrystals of nickel based superalloys. It is found that the bicrystals with smaller misorientation angles contain denser M 23 C 6 but sparse MC particles at grain boundaries, and this kind of bicrystals presents longer stress rupture lives. It was observed that MC carbides were decorated by M 23 C 6 and M 6 C particles at grain boundaries. The formation of these carbide particles, therefore, is likely due to the local fluctuation of chemical composition around MC carbides. In addition, the orientation relationships between MC carbides and γ/γ matrix were also determined. | Xiaoming Dong Xiaoli Zhang Kui Du Yizhou Zhou Tao Jin Hengqiang Ye | 2012 | Journal of Materials Science & Technology2012，28，11： | 4 |
| 12 | Effect of thermal exposure on the microstructure and creep properties of a fourth-generation Ni-based single crystal superalloy显示文摘The effect of thermal exposure on microstructure and creep properties of a fourth-generation nickelbased single crystal superalloy was investigated.The thermal exposure of samples after the full heat treatment was carried out at 1000℃,1100℃ and 1140℃ for 100 h and 200 h.The γ’ coarsening,γ’ rafting and γ channel widening were observed in samples after thermal exposure.When the thermal exposure time was constant,the morphology of γ’ phase in the alloy evolved significantly with increasing aging temperature.The interracial dislocation networks in aged samples after creep ruptured gradually became irregular and sparse with the increase of exposure temperature.When the higher exposure temperature was used,enla rgement of the defect pores was observed in samples,the microcracks were more likely to initiate and propagate at the corner of these pores.After aging at 1000℃ for 100 h,the creep life at 1140℃/137 MPa was slightly longer than that of heat-treated sample,which could be attributed to the slightly coarsened γ’ phase,homogenization of refractor elements.In contrast,the creep life of sample exposed at 1140℃ for 100 h was greatly decreased.The decrease of creep life was dominated by the rafting of γ’phase,the irregular interfacial dislocation networks as well as the enlargement of homogenization pores. | Yeshun Huang Xinguang Wang Chuanyong Cui Zihao Tan Jinguo Li Yanhong Yang Jinlai Liu Yizhou Zhou Xiaofeng Sun | 2021 | Journal of Materials Science & Technology2021，，10： | 4 |
| 13 | On the γ' precipitates of the normal and inverse Portevin-Le Chatelier effect in a wrought Ni-base superalloy显示文摘The Portevin-Le Chatelier(PLC) effects in a wrought Ni-base superalloy with different γ' precipitates contents have been investigated. Detailed analysis on the serration type of the tensile curves indicates that the γ' precipitates have a decisive influence on the transformation from normal to inverse PLC behavior, which is rarely proposed in other works. It is considered that the γ' precipitates play the same role in PLC effect as temperature and strain rate for the investigated wrought Ni-base superalloy. | Xinguang Wang Guoming Han Chuanyong Cui Shuai Guan Jinguo Li Guichen Hou Yizhou Zhou Xiaofeng Sun | 2019 | Journal of Materials Science & Technology2019，35，1： | 3 |
| 14 | Mechanisms of Rhenium on Wettability and Interactions Between Nickel-Base Superalloy Melt and Al2O3-Based Ceramic Material显示文摘A systematic study on the wettability and interactions between superalloy melts with various Re contents and Al2 O3-based ceramic moulds was presented in this paper.It was found that the increase of Re content inhibited the interfacial reactions to some extent.With regard to the 0,1.5 and 3 Re alloys,a double reaction layer containing Al2 O3 and HfO2 was formed at the interface,but the thickness of reaction layer decreased with the increase of Re content.However,only Al2 O3 phase was detected at the interface when the content of Re was 6 wt%,and the interface reaction was the weakest and the thickness of reaction layer was the thinnest.The wetting angle of the alloy/ceramic system increased as the level of Re increased.Moreover,the formation of viscous sand at the interface mainly depended on the change of wetting angle of the system. | Yun Zi Jie Meng Chaowei Zhang Yizhou Zhou Yutian Ding | 2020 | Acta Metallurgica Sinica(English Letters)2020，33，7： | 3 |
| 15 | Effects of Re on surface eutectic formation for Ni-base single crystal superalloys during directional solidification显示文摘Effects of Re on the formation of surface eutectics have been investigated by using Ni-base single crystal superalloys with different Re additions. It was found that Re promotes the segregation of Al and Ta to the eutectic melt, leading to an increase of the surface and internal eutectics. In addition, the addition of Re also increased the freezing range, the local solidification time, and the permeability of the dendritic network within the mushy zone. These factors ultimately promoted the outflow of the interdendritic residual liquid with the action of solidification shrinkage, and led to the formation of more surface eutectics. In contrast, the addition of Re had no obvious influence on the surface eutectic microstructures. | Liang Cao Yizhou Zhou Tao Jin Xiaofeng Sun | 2017 | Journal of Materials Science & Technology2017，33，11： | 3 |
| 16 | Epitaxial growth and oxidation behavior of an overlay coating on a Ni-base single-crystal superalloy by laser cladding显示文摘An overlay coating material was deposited on a single crystal superalloy SRR99 by laser cladding.The microstructure and oxidation behavior of this coating was investigated through scanning electron microscopy(SEM) and X-ray diffraction(XRD). The results indicated that although the composition of the coating was chosen based on the γ' composition in René N5 superalloy, the primary solidification phase of this coating during laser cladding was γ-Ni. Furthermore, under the laser cladding condition, fine parallel dendrites grew epitaxially in the coating from the substrate, indicating the single crystal structure of the substrate was reproduced. When the single crystal MCrAlY coating was oxidized at 1000?, both Al_2O_3 and Al_2O_3 formed during initial oxidation process. As the oxidation time proceeded, the presence of Al_2O_3 facilitated the formation of NiAl_2O_4 spinel oxide. Once the spinel was observed, it flourished and induced some porosity in the scale. When the scale thickness increased to 6–7 μm, large area spallation of the scale began. | Jingjing Liang Yongsheng Liu Jinguo Li Yizhou Zhou Xiaofeng Sun | 2019 | Journal of Materials Science & Technology2019，35，2： | 3 |
| 17 | Portevin-Le Chatelier effect in wrought Ni-based superalloys:Experiments and mechanisms显示文摘The Portevin-Le Chatelier(PLC)effect is a plastic instability in alloys at certain strain rates and deformation temperatures.This plastic instability exhibits serrated yielding in the temporal domain and strain localization in the spatial domain.Wrought Ni-based superalloys often exhibit the PLC effect.To guarantee the safe and stable operation of equipment,it is important to study the PLC effect in wrought Ni-based superalloys.This paper provides a review of various experimental phenomena and micromechanisms related to the PLC effect in wrought Ni-based superalloys,which have been reported in various publications in recent years and include work from our own group.The influences of stacking fault energy andγ’precipitates on the PLC effect in wrought Ni-based superalloys are also discussed in detail.Additionally,several suggestions for the future study of the PLC effect in wrought Ni-based superalloys are provided. | Chuanyong Cui Rui Zhang Yizhou Zhou Xiaofeng Sun | 2020 | Journal of Materials Science & Technology2020，47，16： | 3 |
| 18 | Effect of solution cooling rate on the microstructure and creep deformation mechanism of a rhenium-free second-generation single crystal superalloy显示文摘Various cooling scenarios(water,oil,air and furnace)were employed to study the impacts of the solution cooling rate(SCR)on the microstructure and creep behavior of a novel single-crystal(SX)superalloy.The results showed that the cubic degree and size of theγphases were inversely proportional to the SCR.The creep life first increased and then dropped dramatically with a reduction in the SCR.The creep life of the sample cooled with air cooling(AC)was the highest,up to 144.90 h at 800℃/750 MPa and160.15 h at 1100℃/137 MPa.During creep at 800℃/750 MPa,the improved creep life of the AC sample was mainly attributed to the fine cubicγphases,which decreased the rate ofγ-phase coarsening and favoured plastic deformation by promoting the active movement of dislocations.The AC helped theγphases become rich in Al,Ti and Ta while depleted in Co and Cr,which enhanced its stacking fault energy,thus promoting the formation of dislocation locks.Meanwhile,the largest negative lattice misfit caused by AC induced denserγ/γinterface dislocation networks at 1100℃/137 MPa,which efficiently reduced the minimum creep rate.The calculated average dislocation spacing results indicated that the smallest density of excess dislocations corresponded to the AC sample,proving its greatest creep resistance.Interestingly,the size of the secondaryγphases first decreased and then increased sharply with decreasing SCR during creep at 1100℃/137 MPa,when fine secondaryγphases had a positive role in the blockage of dislocation movement in the matrix.Eventually,the comprehensive SCR effect was explored to provide more guidance in the design of Re-free SX superalloys. | Xipeng Tao Yunling Du Xinguang Wang Jie Meng Yizhou Zhou Jinguo Li Xiaofeng Sun | 2022 | Journal of Materials Science & Technology2022，，36： | 3 |
| 19 | Variation of crystal orientation during epitaxial growth of dendrites by laser deposition显示文摘A nickel-based superalloy was deposited onto a single crystal substrate based on epitaxial laser metal forming(E-LMF). The microstructure development in two depositions has been researched. For the first time, the crystal orientation of dendrites varying beyond 20° was found when the dendrites deflected in deposition. In addition, a new grain boundary was found between different orientation dendrites in a grain, and the detected grain boundary angle was 23°. The result shows that flowing field in laser pool is responsible for this phenomenon. | Guowei Wang Jingjing Liang Yizhou Zhou Libin Zhao Tao Jin Xiaofeng Sun | 2018 | Journal of Materials Science & Technology2018，34，4： | 3 |
| 20 | Effect of Solidifcation Rate on Grain Structure Evolution During Directional Solidifcation of a Ni-based Superalloy显示文摘The effect of solidification rate on grain structure evolution during directional solidification(DS) of a Ni-based superalloy was explored.It was found that a high solidification rate led to sharper <001> texture and smaller grain size in the DS samples.One of the most important findings in this work was that such result was not in accordance with the general concept,and the sharper <001> texture was accompanied by the larger grain size.To explain the contradiction,the modeling samples with five grains were produced and the effect of solidification rate on the evolution of grain texture was illustrated based on the modeling samples. | Xiaoli Zhang Yizhou Zhou Tao Jin Xiaofeng Sun Lin Liu | 2013 | Journal of Materials Science & Technology2013，29，9： | 2 |
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