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| 1 | Geochemistry of Two Types of Basalts in the Emeishan Basaltic Province: Evidence for Mantle Plume-Lithosphere Interaction显示文摘Based on the temporal-spatial distribution and geochemical characteristics, the Emeishan basalts can be divided into two types: high-P2O-TiO2 basalt (HPT) and low-P2O5-TiO2 basalt (LPT), which differ distinctly in geochemistry: the LPTs are characterized by relatively high abundances of MgO, total FeO and P2O5 and compatible elements (Cr, Ni, Sc), and relatively low contents of moderately compatible elements (V, Y, Yb, Co), LREE and other incompatible elements compared with the HPT. On the diagrams of trace element ratios, they are plotted on an approximately linear mixing line between depleted and enriched mantle sources, suggesting that these two types of basalts resulted from interactions of varying degrees between mantle plume and lithospheric mantle containing such volatile-rich minerals as amphibole and apatite. The source region of the LPT involves a smaller proportion of lithospheric components, while that of the HTP has a larger proportion of lithospheric components. Trachyte is generated by partial melting of the basic igneous rocks at the base of the lower continental crust. Both the two types of magmas underwent certain crystal fractionation and contamination of the lower crust at high-level magma chambers and en route to the surface. | ZHANG Zhaochong (张招崇) WANG Fusheng(王福生) | 2002 | Acta Geologica Sinica(English Edition)2002，76，2： | 31 |
| 2 | Synthesis and Structure of A Novel Caged Bicyclic Phosphate Flame Retardant显示文摘A novel caged bicyclic phosphate flame retardant tri(1-oxo-2,6,7-trioxa-l-phosphabicyclo [2.2.2] octane-methyl) phosphate (Trimer) was synthesized from 1-oxo-4-hydroxymethyl-2,6,7-trioxa-l-phosphabicyclo [2.2.2] octane (PEPA) and phosphorus oxychloride in this paper. Its structure was characterized by elemental analysis, FTIR, 1H NMR, 31P NMR and X-ray diffraction analysis. | Li, X Ou, YX Zhang, YH Lian, DJ | 2000 | Chinese Chemical Letters2000，11，10： | 28 |
| 3 | Superluminal and Negative Group Velocity in the Electromagnetic Wave Propagation显示文摘In this paper, a penetrating analysis is first made of the superluminal and negative group velocities that occur in the EM wave propagation. Discussed then are the superluminal and negative group velocities which are in the state of evanescent waves in the waveguide below cutoff(WBCO).Through an experiment in the coaxial photonic crystal a group velocity of 1.5-2.4 times the speed of light are observed in the stop band. | Huang Zhixun, Lu Guizhen, Guan Jian (Department of Communication Engineering, Beijing Broadcasting Institute, Beijing 100024) | 2003 | 工程科学(英文版)2003，1，2： | 18 |
| 4 | 一种基于ASP.NET的自定义报表的设计与实现显示文摘本文对ASP.NETWeb应用程序中的自定义报表进行了研究,提出了一种自定义Web报表模型。通过Crys-talReports引擎和ADO.NET对报表底层接口进行控制,完全实现了对报表的自定义,解决了Web应用程序中自定义报表的实现问题。 | 陈传波 黄刚 刘清慧 | 2006 | 计算机工程与科学2006，28，6： | 17 |
| 5 | N-亚水杨基苄胺过渡金属配合物的合成、结构与抑菌性能研究(英文)显示文摘N-salicylidene-benzylamineato M(Ⅱ) complexes (ZnL2, CuL2 and CdL2) were synthesized, characterized and valued for antimicrobial activities against bacterial strands using the agar diffusion method. The crystal of ZnL2 was determined by X-ray diffraction. It crystallizes in the Monoclinic system, space group C2/c with a=2.269 1(3), b=0.918 2(1), c=1.239 5(2) nm, β=117.89(2), Z=4, R1=0.049 4, wR2=0.138 2. The complexes were found to be active against Staphylococcus aureus and Eschierichia Coli. CCDC: 249474. | 许兴友 高健 陈军 李善忠 杨绪杰 李一志 刘永江 | 2005 | 无机化学学报2005，21，5： | 15 |
| 6 | Properties and characterization of Au^(3+)-adsorption by mycelial waste of Streptomyces aureofaciences显示文摘Mycelial waste of Streptomyces aureofaciences procured from the aureomycin fermentation industry is used as biosorbent for Au3+. The properties of Au3+ adsorption by the mycelial waste are studied. The results indicate that the optimum pH value of Au3+ adsorption is 3.5. The biosorption is a rapid and non-temperature-dependent process. The bio-sorptive capacity with 45.6 mg/g and efficiency with 91.2% are achieved under the conditions of pH 3.5 and 30℃ for 45 min, in which the ratio is 50 mg/g dry weight for the concentrations of initial Au3+ and the mycelial waste. The Au3+ ions adsorbed on the mycelial waste can be eluted. The observation in a transmission electron microscope shows that the Au3+ ions can be reduced to Au particles by the mycelial waste and the Au can become gold crystals with differentforms and sizes. X-ray photoelectron spectroscopy analysis further proves that the Au3+ can be reduced to Au0 by the mycelial waste. | LIU Yueying, FU Jinkun, HU Hongbo, TANG Dingliang, Nl Zimian & YU Xinsheng1. Department of Biology, 2. State Key Laboratory for Physical Chemistry of Solid Surface, 3. Center for Analysis & Testing, Xiamen University, Xiamen 361005, China | 2001 | Chinese Science Bulletin2001，46，20： | 15 |
| 7 | THE EFFECT STRESS ON THE MAGNETOSTRICTION IN TWIN- FREE SINGLE CRYSTALS Tb_y Dy_(1-y) (Fe_(1-x) T_x)_2 (T=Al,Mn)显示文摘Magnetostriction at room temperature under various conditions of compressive prestress and applied fields in Tb yDy 1-y (Fe 1-x T x) 2 (T=Al,Mn) twin-free single crystals were investigated. The substitution of Al or Mn for Fe lowers the magnetostriction un-der ordinary temperature and pressure, but it also decreases the saturation field, which enables these materials with potential benefits for applications. | Y.X.Li, G.Z.Xu,J.P.Qu, F.G.Liu and B.W. Wang Hebei University of Technology, Tianjin 300130, China C. Zhao Tianjin University, Tianjin 300072, China S.X. Gao Hebei Normal University,Shijiazhuang 050091, China C.C. Tang, G.H.Wu, J.H.Wang, J.Du and W | 1999 | Acta Metallurgica Sinica(English Letters)1999，12，5： | 14 |
| 8 | Water contents and deformation mechanism in ductile shear zone of middle crust along the Red River fault in southwestern China显示文摘Using Fourier transform infrared spectroscopy (FTIR), we measured water contents of quartz and feldspar for four thin sections of felsic mylonite and two thin sections of banded granitic gneiss col- lected from a ductile shear zone of middle crust along the Red Rivers-Ailaoshan active fault. The ab- sorbance spectra and peak position suggest that water in quartz and feldspar of granitic gneiss and felsic mylonite occurs mainly as hydroxyl in crystal defect, but also contains inclusion water and grain boundary water. The water contents of minerals were calculated based on the absorbance spectra. Water content of feldspar in granitic gneiss is 0.05 wt%-0.15 wt%, and that of quartz 0.03 wt%-0.09 wt%. Water content of feldspar ribbon and quartz ribbon in felsic mylonite is 0.095 wt%-0.32 wt%, and those of fine-grained feldspar and quartz are 0.004 wt%-0.052 wt%. These data show that the water content of weakly deformed feldspar and quartz ribbons is much higher than that of strongly deformed fine-grained feldspar and quartz. This suggests that strong shear deformation leads to breakage of the structures of constitutional water, inclusion and grain boundary water in feldspar and quartz, and most of water in minerals of mylonite is released to the upper layer in the crust. | ZHOU YongSheng HE ChangRong YANG XiaoSong | 2008 | Science China Earth Sciences2008，51，10： | 14 |
| 9 | Effect of long term aging on microstructure and stress rupture properties of a nickel based single crystal superalloy | Zhenxue Shi Jiarong Li Shizhong Liu | 2012 | Progress in Natural Science:Materials International2012，22，5： | 14 |
| 10 | 一维链状4-羧基苯氧乙酸桥联钴配位聚合物[Co(p-CPOA)(2,2'-bipy)(H_2O)]_n的合成与晶体结构显示文摘A novel coordination polymer of [Co( p-CPOA)(2,2′-bipy)(H2O)]n ( p-CPOA2-=4-carboxylphenoxyacetate dianion, 2,2′-bipy=2,2′-bipyridine) was synthesized and characterized by elemental analysis, IR and X-ray single crystal diffraction. The title complex crystallizes in monoclinic space group C2/c, with a=1.424 4(3) nm, b=1.316 6(3) nm, c=1.947 7(4) nm, β=104.56(3)°. V=3.535 3(14) nm3, Z=8, R=0.028 5, wR=0.089 1. The cobalt(Ⅱ) ion displays a distorted octahedral coordination geometry, defined by three carboxyl oxygen atoms from different p-CPOA2- groups, two nitrogen atoms from 2,2′-bipyridine ligand and one water molecule. The cobalt atoms are bridged by p-CPOA2- groups, forming a one-dimensional chain structure along a axis. The adjacent Co...Co atoms distance is 0.996 8 nm. A layer supramolecular network is contrsucted by the hydrogen bonds and π-π stacking interactions. CCDC: 220039. | 高山 霍丽华 谷长生 赵辉 赵经贵 | 2005 | 无机化学学报2005，21，5： | 13 |
| 11 | 基于.NET平台的Web报表打印方法研究显示文摘文中介绍了基于ASP .NET技术的Web报表打印方法 ,对每一种方法都进行了详细阐述 ,并且分析了每种方法的优缺点 ,相信会对解决Web报表打印问题有一定的借鉴意义。 | 崔亮 郭忠文 | 2003 | 计算机应用2003，23，z2： | 12 |
| 12 | A METHOD OF PREPARING SPHERICAL NANO-CRYSTAL CELLULOSE WITH MIXED CRYSTALLINE FORMS OF CELLULOSE Ⅰ AND Ⅱ显示文摘A new kind of nano-crystal cellulose (NCC) prepared from natural cotton fiber has been obtained by the method of acid hydrolysis. Compared to most other nanophase materials that derive from inorganic materials, our products are prepared from natural cotton fibers. The products are of spherical shape with mixed crystal forms of cellulose Ⅰ and Ⅱ. The preparation conditions determine the properties of the products. Prior treatment is a critical procedure. The properties of the products are also strongly affected by such conditions as the kinds of acids used, the ratio of the acid mixture, the acid concentration, the ultrasonic agitation time and hydrolysis temperature. The number average molecular weight of NCC is determined by gel permeation chromatography (GPC). The particle size and shape were determined by transmission electron microscopy (TEM). X-ray diffraction was used to detect the crystallinity and average crystallite size of the particle. | Xiao-fang Li En-yong Ding Guo-kang Li Laboratory of Cellulose and Lignocellulosics Chemistry, Guangzhou Institute of Chemistry, Chinese Academy of Sciences, Guangzhou 510650 China College of Material Science and Engineering South China University of Technology, Guangzhou 510641, China | 2001 | Chinese Journal of Polymer Science2001，19，3： | 12 |
| 13 | Microstructure evolution of single crystal copper wires in cold drawing显示文摘The deformation microstructure evolution of single crystal copper wires produced by OCC method has been studied with the help of TEM, EBSD and OM. The results show that there are a small number of dendrites and twins in the undeformed single crystal copper wires. However, it is difficult to observe these dendrites in deformed single crystal copper wires. The structure evolution of deformed single crystal copper wires during drawing process can be divided into three stages. When the true strain is lower than 0.94, macroscopic subdivision of grains is not evident, and the microscopic evolution of deformed structure is that the cells are formed and elongated in drawn direction. When the true strain is between 0.94 and 1.96, mac- roscopic subdivision of grains takes place, and the number of microbands located on {111} and cell blocks is much more than that with the true strain lower than 0.94. When the true strain is larger than 1.96, the macroscopic subdivision of grains becomes more evident than that with the true strain between 0.94 and 1.96, and S-bands structure and lamellar boundaries will be formed. From EBSD analysis, it is found that part of <100> texture resulting from solidifying is transformed into <111> and <112> due to shear deformation, but <100> texture component is still kept in majority. When the true strain is 0.94, the misorientation angle of dislocation boundaries resulting from deformation is lower than 14°. However, when the true strain arrives at 1.96, the misorientation angle of some boundaries will be greater than 50°, and the peak of misorientation angle distribution produced by texture evolution is located in the range between 25° and 30°. | CHEN Jian1,2, YAN Wen1,2, WANG XueYan2 & FAN XinHui2 1 Department of Applied Physics, Northwestern Polytechnical University, Xi’an 710072, China 2 School of Material Science and Chemical Engineering, Xi’an Technological University, Xi’an 710032, China | 2007 | Science China(Technological Sciences)2007，50，6： | 10 |
| 14 | Hierarchical ZSM-11 with intergrowth structures:Synthesis,characterization and catalytic properties显示文摘Hierarchical ZSM-11 microspheres with intercrystalline mesoporous properties and rod-like crystals intergrowth morphology have been synthesized using a spot of tetrabutylammonium as a single template.XRD,FTIR,SEM,TEM and N2 adsorption analysis revealed that each individual particle was composed of nanosized rod crystals inserting each other and the intercrystalline voids existing among rods gave a significant mesopore size distribution.Steam treatment result demonstrated the excellent hydrothermal stability of samples.Various crystallization modes including constant temperature crystallization (one-stage crystallization) and two-stage temperature-varying crystallization with different 1st stage durations were investigated.The results suggested that the crystallization modes were mainly responsible for the adjustable particle size and textural properties of samples while the small amount of tetrabutylammonium bromide was mainly used to direct the formation of both ZSM-11 framework and its intergrowth morphology.Furthermore,the performance of optimal ZSM-11 as an active component for the catalytic pyrolysis of heavy oil was also investigated.Compared with the commercial pyrolysis catalyst,the hierarchical ZSM-11 catalyst exhibited a high selectivity to desired products(LPG+gasoline+diesel),as well as a much lower dry gas and coke yield,plus a high selectivity and yield of light olefins(C=3 C=4)and very poor selectivity to benzene.Therefore,fully open micropore-mesopore connectivity would make such hierarchically porous ZSM-11 zeolites very attractive for applications in clean petrochemical catalysis field. | Qingjun Yu Chaoyue Cui Qiang Zhang Jing Chen Yang Li Jinpeng Sun Chunyi Li Qiukai Cui Chaohe Yang Honghong Shan | 2013 | Journal of Energy Chemistry2013，22，5： | 10 |
| 15 | Research on crystal growth and properties of a new nonlinear optical crystal:Bismuth borate BiB_3O_6显示文摘BiB3O6 (BIBO) single crystals with sizes of 44 mm × 24 mm × 10 mm and weight of 24.7 g have been successfully grown by the top-seeded method. In this note, the preparation of seed, the growth of crystal and some problems encountered are reported. The lattice parameters of BIBO are a =7.1203(7)A, b = 4.9948(7)A, c = 6.5077(7)A, β= 105.586(8) ', V=222.93(5)A3, which were determined by BRUKER-P4 four-circle diffractometer. BIBO is biaxial crystal and the relative orientation of (X, Y, Z) with regard to (a, b, c) is: X|| b, (Y, c) =47.2°, (Z, a) = 31.6°, determined by the X-ray analysis combined with polarized microscopy. The second-harmonic-generation (SHG) conversion efficiency of the sample for 1.064 μm light is up to 67.7%. We have also obtained the third harmonic generation (THG) of 1.064 μm, namely, 1.064 μm + 0.532 μn →0.355 μm. BIBO crystal is free of moisture and hygroscopy. | TENG Bing, WANG Jiyang, WANG Zhengping, JIANG Huaidong, SONG Renbo, LIU Hong, HU Xiaobo, LIU Yaogang, WEI Jingqian & SHAO ZongshuState Key Laboratory of Crystal Materials, Shandong University, Ji’nan 250100, China | 2001 | Chinese Science Bulletin2001，46，21： | 10 |
| 16 | TFT-LCD玻璃基板材料性能与生产特点显示文摘薄膜晶体管液晶显示器(Thinfilm transistor liquid crystal display,TFT—LCD)的兴起为TFT-LCD玻璃提供了巨大的市场需求。作为TFT—LCD的消费大国,中国也正在成为TFT—LCD显示器件的生产大国,在此背景下,国内TFT—LCD玻璃生产设施的建设也将成为必然。 | 陆丹 徐刚 | 2011 | 新材料产业2011，，9： | 10 |
| 17 | Effect of hierarchical ZSM-5zeolite crystal size on diffusion and catalytic performance of n-heptane cracking显示文摘Hierarchical ZSM-5zeolite aggregates with different sizes of nanocrystals were synthesized using different amounts of the mesoporogen 3-aminopropyl- triethoxysilane.The effect of the crystal size on the catalytic cracking of n-heptane was investigated and the Thiele modulus and effectiveness factor were used to determine the reaction rate-limiting step.The crystal size affected the textual properties of the catalysts but not the acidic properties of the catalysts.The reaction rate was first order with respect to the n-heptane concentration.Cracking over hierarchical zeolites with nanocrystal sizes larger than about 50nm took place under transition-limiting conditions,whereas the reaction over hierarchical zeolites with nanocrystal sizes of 15 or 30nm proceeded under reaction control conditions.Hierarchical ZSM-5 zeolite aggregates with smaller nanocrystals had better selectivity for light olefins which can be ascribed to the shorter diffusion path lengths and lower diffusion resistance in these catalysts. Furthermore,these catalysts had lower coking levels which can be attributed to the substantial number of mesopores which prevent the formation of coke precursors. | Shuman Xu Xiaoxiao Zhang Dangguo Cheng Fengqiu Chen Xiaohong Ren | 2018 | Frontiers of Chemical Science and Engineering2018，12，4： | 10 |
| 18 | Rapid growth of ternary eutectic un der high undercooling conditions显示文摘Rapid solidification of bulk Ag42.4Cu21.6Sb36 ternary eutectic alloy is accomplished by glass fluxing method,during which the maximum undercooling attains 114 K (0.16 TE). Under high undercooling conditions,the ternary eutectic consists ofε (Ag3Sb),(Sb)and θ(Cu2Sb)phases,instead of (Ag),(Sb)and θphases as predicted by the phase diagram.In the sample of small undercooling,the alloy microstructure is characterized by the mixture of primary θ(Cu2Sb),(ε+θ) and (ε+Sb) pseudobinary eutectics,and regular (ε+θ+Sb) ternary eutectic.With the increase of undercooling, θ (Cu2Sb) primary phase and pseudobinary eutectics disappear gradually,and ternary eutectic transfers from regular to anomalous structure.When undercooling exceeds 102 K,anomalous (ε+θ+Sb) ternary eutectic is the unique microstructure.Competitive nucleation and growth of these three eutectic phases is the main cause for the formation of complex growth morphologies.Based on the current experiments and theoretical calculations,it can be concluded that the intermetallic compound phaseθ(Cu2Sb) is the leading nucleating phase. | RUAN Ying CAO Chongde WEI Bingbo | 2004 | Science China(Physics,Mechanics & Astronomy)2004，47，6： | 10 |
| 19 | Crystal Ball仿真软件的探讨及其在微机上的应用显示文摘文章围绕Crystal Ball仿真软件的应用问题,阐述了在人们分析随机和复杂系统的过程时,仿真技术是必不可少的工具之一。文章描述了仿真技术的主要研究步骤以及Crystal BalI仿真软件的主要功能、应用方法,文章说明了该软件对于仿真技术的普及起到的重要作用。 | 马慧 | 2004 | 计算机系统应用2004，13，9： | 9 |
| 20 | Bi2O3晶体结构和氧缺陷协同作用:促进中间产物的吸附活化、转化途径和光催化反应效率显示文摘在两种不同晶体结构的Bi2O3表面构造了人工氧缺陷,采用实验与模拟计算相结合的方法,从分子层面证实了特定晶体结构和氧缺陷的协同作用可以提高光催化效率,并有效调控光催化转化NO的反应路径,进而加快了整个反应历程.优化后的α-Bi2O3-X可见光净化NO去除率从7.3%增长至20.1%,而β-Bi2O3-X可见光光催化性能从25.2%提高至52.0%,活性增强的差异与不同的晶体结构、氧缺陷有关. DFT计算和实验结果证实,α-Bi2O3和β-Bi2O3表面氧缺陷作为活化中心,促进反应物和中间产物的吸附活化.同时,晶体结构和氧缺陷协同调控电子传递途径,原子排布呈隧道结构的氧缺陷β-Bi2O3对反应物活化以及电荷转移效率比Z型原子排布的氧缺陷α-Bi2O3更高效,这归因于在α-Bi2O3和β-Bi2O3表面构建的缺陷结构不同.原位FT-IR揭示了光催化氧化NO的反应机理,不同晶相的Bi2O3光催化NO转换途径可以由不同的表面缺陷结构进行有效调控. | 雷奔 崔文 盛建平 王红 陈鹏 李解元 孙艳娟 董帆 | 2020 | Science Bulletin2020，65，6： | 9 |
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