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| 1 | Trace bis-(3-sulfopropyl)-disulfide enhanced electrodeposited copper foils显示文摘Smooth and strong copper foils are highly required for the development of printed circuit boards and Li-ion batteries.Adding additives is an efficient and low-cost method to enhance electrodeposited copper foils.Here we chose Bis-(3-sulfopropyl)-disulfide(SPS)as the additive and investigated its concentration on the surface roughness and tensile strength of the electrodeposited copper foils.A copper foil with the smoothest surface(Rz=2.1μm)and the highest tensile strength(~338 MPa)was prepared with1.5 mg/L SPS.The contact angle on the copper foil decreased with the reduction of surface roughness.The enhancing mechanism of the SPS was investigated by scanning electron microscopy and X-ray diffraction.The refined grain and enhanced(220)texture were considered to be the radical reason for the smooth and strong copper foils.The electrochemical results prove the suppressing effect is related to the SPS adsorption. | Lingling Liu Yeqiang Bu Yue Sun Jianfeng Pan Jiabin Liu Jien Ma Lin Qiu Youtong Fang | 2021 | Journal of Materials Science & Technology2021，，15： | 6 |
| 2 | A compact design of four-degree-of-freedom transmission electron microscope holder for quasi-four-dimensional characterization显示文摘Electron tomography(ET) has been demonstrated to be a powerful tool in addressing challenging problems, such as understanding 3 D interactions among various microstructures. Advancing ET to broader applications requires novel instrumentation design to break the bottlenecks both in theory and in practice. In this work, we built a compact four-degree-of-freedom(threedirectional positionings plus self-rotation) nano-manipulator dedicated to ET applications, which is called X-Nano transmission electron microscope(TEM) holder. All the movements of the four degrees of freedom are precisely driven by built-in piezoelectric actuators, minimizing the artefacts due to vibration and drifting of the TEM stage. Full 360° rotation is realized with an accuracy of 0.05° in the whole range, which solves the missing wedge problem. Meanwhile, the specimen can move to the rotation axis with an integrated 3D nano-manipulator, greatly reducing the effort in tracking sample locations during tilting.Meanwhile, in-situ stimulation function can be seamlessly integrated into the X-Nano TEM holder so that dynamic information can be uncovered. We expect that more delicate researches, such as those about 3D microstructural evolution, can be carried out extensively by means of this holder in the near future. | ZHANG YiZhi BU YeQiang FANG XiaoYang WANG HongTao | 2020 | Science China(Technological Sciences)2020，63，7： | 3 |
| 3 | The Msi1-mTOR pathway drives the pathogenesis of mammary and extramammary Paget’s disease显示文摘Mammary and extramammary Paget’s Diseases(PD)are a malignant skin cancer characterized by the appearance of Paget cells.Although easily diagnosed,its pathogenesis remains unknown.Here,single-cell RNA-sequencing identified distinct cellular states,novel biomarkers,and signaling pathways—including mTOR,associated with extramammary PD.Interestingly,we identified MSI1 ectopic overexpression in basal epithelial cells of human PD skin,and show that Msi1 overexpression in the epidermal basal layer of mice phenocopies human PD at histopathological,single-cell and molecular levels.Using this mouse model,we identified novel biomarkers of Paget-like cells that translated to human Paget cells.Furthermore,single-cell trajectory,RNA velocity and lineage-tracing analyses revealed a putative keratinocyte-to-Paget-like cell conversion,supporting the in situ transformation theory of disease pathogenesis.Mechanistically,the Msi1-mTOR pathway drives keratinocyte-Paget-like cell conversion,and suppression of mTOR signaling with Rapamycin significantly rescued the Paget-like phenotype in Msi1-overexpressing transgenic mice.Topical Rapamycin treatment improved extramammary PD-associated symptoms in humans,suggesting mTOR inhibition as a novel therapeutic treatment in PD. | Yongli Song Christian F.Guerrero-Juarez Zhongjian Chen Yichen Tang Xianghui Ma Cong Lv Xueyun Bi Min Deng Lina Bu Yuhua Tian Ruiqi Liu Ran Zhao Jiuzhi Xu Xiaole Sheng Sujuan Du Yeqiang Liu Yunlu Zhu Shi-jun Shan Hong-duo Chen Yiqiang Zhao Guangbiao Zhou Jianwei Shuai Fazheng Ren Lixiang Xue Zhaoxia Ying Xing Dai Christopher J.Lengner Bogi Andersen Maksim V.Plikus Qing Nie Zhengquan Yu-Show | 2020 | Cell Research2020，30，10： | 2 |
| 4 | Room-temperature plasticity in diamond显示文摘In spite of extremely high strength and hardness, the property of brittleness is tightly linked to diamond. In the deformation of diamond at room temperature, the plasticity of the diamond is normally considered hard to occur because of the domination of catastrophic brittle fracture. Herein, we employed in-situ transmission electron microscopy to reveal the diamond roomtemperature plastic behavior, and compared it with a recent report(Adv. Mater. 2020, 1906458) on transformation-induced room-temperature plasticity of diamond nanopillars. Our present in-situ uniaxial compression tests in sub-micron-sized diamond pillars indicate that the plasticity in diamond is carried out by dislocations slipping instead of phase transformation and the initiation of plasticity highly depends on the stress state. On the other hand, we noted that a high proportion of amorphous surface layer in the diamond pillars with a diameter of less than 20 nm may be a significant factor leading to the plasticity. | BU YeQiang WANG Peng NIE AnMin WANG HongTao | 2021 | Science China(Technological Sciences)2021，64，1： | 0 |
| 5 | Natural overlaying behaviors push the limit of planar cyclic deformation performance in few-layer MoS_(2)nanosheets显示文摘As a typical two-dimensional(2D)transition metal dichalcogenides(TMDCs)material with nonzero band gap,MoS_(2)has a wide range of potential applications as building blocks in the field of nanoelectronics.The stability and reliability of the corresponding nanoelectronic devices depend critically on the mechanical performance and cyclic reliability of 2D MoS_(2).Although an in situ technique has been used to analyze the mechanical properties of 2D materials,the cyclic mechanical behavior,that is,fatigue,remains a major challenge in the practical application of the devices.This study was aimed at analyzing the planar cyclic performance and deformation behavior of three-layer MoS_(2)nanosheets(NSs)using an in situ transmission electron microscopy(TEM)variable-amplitude uniaxial low-frequency and cyclic loading-unloading tensile acceleration test.We also elucidated the strengthening effect of the natural overlaying affix fragments(other external NSs)or wrinkle folds(internal folds from the NS itself)on cycling performances and service life of MoS_(2)NSs by delaying the whole process of fatigue crack initiation,propagation,and fracture.The results have been confirmed by molecular dynamics(MDs)simulations.The overlaying enhancement effect effectively ensures the long-term reliability and stability of nanoelectronic devices made of few-layer 2D materials. | Peifeng Li Guangjie Zhang Zhuo Kang Xin Zheng Yong Xie Chunyuan Liang Yizhi Zhang Xiaoyang Fang Rong Sun Zhiquan Liu Yeqiang Bu Yang Lu Yue Zhang | 2023 | InfoMat2023，5，9： | 0 |
| 6 | Enhanced plastic deformation capacity in hexagonal-close-packed medium entropy alloys via facilitating cross slip显示文摘Alloys with a hexagonal close-packed(HCP)lattice often suffer from intrinsic brittleness due to their in-sufficient number of slip systems,which limits their practical uses.In this paper,nevertheless,we show that remarkably tensile ductility in HCP Hf-Zr-Ti medium entropy alloys(MEAs)was achieved,particu-larly in the MEAs with a higher content of Hf.Both first-principles calculation and experimental analyses reveal that addition of Hf increases basal I2 stacking fault energy and decreases prismatic stacking fault energy in these HCP MEAs,which promotes the source of pyramidal dislocations due to the facilitated cross slips of basal dislocations and eventually give rise to the observed large tensile ductility.Our current findings not only shed new insights into understanding deformation of HCP alloys,but also provide a basis for controlling alloying effects for developing novel HCP complex alloys with optimized properties. | Xiaocan Wen Hailong Huang Honghui Wu Meisa Zhou Yeqiang Bu Xiaoyuan Yuan Suihe Jiang Hui Wang Xiongjun Liu Hongtao Wang Jiabin Liu Yuan Wu Zhaoping Lu | 2023 | Journal of Materials Science & Technology2023，，3： | 0 |
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